20种农药混标/GB/T 39665-2020|西域试剂

20种农药混标/GB/T 39665-2020,标准溶液,溶剂:甲醇, 不同浓度

产品编号：西域质检-81518

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货号	包装	价格	库存与货期	购买量	操作
西域质检-81518		￥530.00	杭州北京（现货）

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甲醇中20种农药混标

CAS号	名称	标准值	单位
63-25-2	甲萘威	100	μg/mL
10605-21-7	多菌灵	50	μg/mL
2303-16-4	燕麦敌	500	μg/mL
1420-07-1	草消酚	100	μg/mL
330-54-1	敌草隆	500	μg/mL
133855-98-8	氟环唑	100	μg/mL
67564-91-4	丁苯吗啉	100	μg/mL
79241-46-6	精吡氟禾草灵	10	μg/mL
103361-09-7	丙炔氟草胺	1000	μg/mL
1689-83-4	碘苯腈	100	μg/mL
36734-19-7	异菌脲	1000	μg/mL
141112-29-0	异恶唑草酮	500	μg/mL
143390-89-0	醚菌酯	500	μg/mL
330-55-2	利谷隆	500	μg/mL
2212-67-1	禾草敌	100	μg/mL
6923-22-4	久效磷	50	μg/mL
2312-35-8	炔螨特	1000	μg/mL
139-40-2	扑灭津	50	μg/mL
122-34-9	西玛津	100	μg/mL
24602-86-6	十三吗啉	100	μg/mL

甲醇中20种农药混标

备注：氟环唑 133855-98-8，标准中为106325-08-0，该CAS号已被133855-98-8替代；

丁苯吗啉 67564-91-4，标准中为67306-03-0，该CAS号已被67564-91-4替代。

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO 9001.

Product Name(产品名称) 20 Pesticide Mix in Methanol,10µg/mL,50µg/mL,100µg/mL,500µg/mL,1000µg/mL(甲醇中20种农药混标)

Part Number(产品编号) 81518

Lot Number(产品批号) -

Expiry Date(失效日期) 2029-Oct-30________________________________________________

Storage(存储条件) (2~8)℃,Keep in the shade
冷藏(2~8)℃,置于阴凉处

CERTIFIED
Component No. (组分数)	Peak Sequence (出峰顺序)	Component (组分)	CAS No.	Concentration (μg/mL) (浓度)	Relative Expanded Uncertainty(%) (k=2) (相对扩展不确定度)
1	1	Carbendazim (多菌灵)	10605-21-7	50	4
2	2	Monocrotophos (久效磷)	6923-22-4	50	4
3	3	Simazine (西玛津)	122-34-9	100	3
4	4	Carbaryl (甲萘威)	63-25-2	100	3
5	5	Fenpropimorph (丁苯吗啉)	67564-91-4	100	3
6	6	Diuron (敌草隆)	330-54-1	500	3
7	7	Propazine (扑灭津)	139-40-2	50	4
8	8	Tridemorph (十三吗啉)	24602-86-6	100	3
9	9	Linuron (利谷隆)	330-55-2	500	3
10	10	Flumioxazin (丙炔氟草胺)	103361-09-7	1000	2
11	11	Molinate (禾草敌)	2212-67-1	100	3
12	12	Isoxaflutole (异恶唑草酮)	141112-29-0	500	3
13	13	Epoxiconazole (氟环唑)	133855-98-8	100	3
14	14	Iprodione (异菌脲)	36734-19-7	1000	2
15	15	Kresoxim-methyl (醚菌酯)	143390-89-0	500	3
16	16	Diallate (燕麦敌)	2303-16-4	500	3
17	17	Fluazifop-P-Butyl (精吡氟禾草灵)	79241-46-6	10	5
18	18	Propargite (炔螨特)	2312-35-8	1000	2
19	19	Ioxynil1 (碘苯腈)	1689-83-4	100	3
20	20	Dinoterb1 (草消酚)	1420-07-1	100	3

C H R O M A T O G R A M

Note:

See the attachment below for the MRM mode. 关于MRM模式，请参阅下面的附件。

1. Ioxynil (CAS No. : 1689-83-4) and Dinoterb (CAS No. : 1420-07-1) were dectected by LC-MS/MS with negative ion mode.(碘苯腈（CAS No. : 1689-83-4）和草消酚（CAS No. : 1420-07-1）采用负离子模式LC-MS/MS检测)

Instrument(检测仪器) HPLC-MS/MS

Column(色谱柱) C18(2.1x50mm,1.8μm)

Column Oven(柱温) 35℃

Method Details(方法参数)
A: 0.1% Formic Acid(0.1甲酸)
B: Acetonitrile(乙腈)

Time/min	A/%	B/%
0.00	95	5
2.00	95	5
8.00	40	60
11.00	5	95
13.00	5	95
13.01	95	5
15.00	95	5

Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of preparation, purity of neat materials, homogeneity, stability testing.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards. The calibration of the balances is verified annually by an external accredited calibration service. This analysis method has been verified using an approach consistent with ISO 17034:2016 & ISO 17025:2017.

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity consistent with ISO 17034.

Storage

The RM should be stored in the original sealed bottle at the indicated temperature.